1,2,2,6,6-Pentamethyl-4-piperidone → 1,2,2,6,6-Pentamethyl-piperidin-4-one oxime

HRID 1630425

反応式

HRID 1630425 の反応式
[CH3:1][N:2]1[C:7]([CH3:9])([CH3:8])[CH2:6][C:5](=O)[CH2:4][C:3]1([CH3:12])[CH3:11].Cl.[NH2:14][OH:15]>>[CH3:1][N:2]1[C:7]([CH3:9])([CH3:8])[CH2:6][C:5](=[N:14][OH:15])[CH2:4][C:3]1([CH3:12])[CH3:11]

参加物

3

反応物 2

HCID 2419551,2,2,6,6-Pentamethyl-4-piperidoneHCID 443297Hydroxyamine hydrochloride

生成物 1

HCID 2419501,2,2,6,6-Pentamethyl-piperidin-4-one oxime

実験手順

1,2,2,6,6-Pentamethyl-piperidin-4-one oxime was prepared from 1,2,2,6,6-pentamethyl-piperidin-4-one and hydroxylamine hydrochloride using conditions of General Method 1. 1H NMR (250 MHz, CHLOROFORM-d) δ 2.52 (2H, s), 2.28 (3H, s), 2.21 (2H, s), 1.12 (6H, s), 1.11 (6H, s).

出典と根拠

ORDレコード
ord-42de69c812594161917278938c1f29b2
出典データセット
uspto-grants-2014_07
特許番号
US08791134B2

関連ノート

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