Tert-butyl 4-isopropyl-2-nitrophenylcarbamate → Tert-butyl 2-amino-4-isopropylphenylcarbamate
反応式
[C:1]([O:5][C:6](=[O:20])[NH:7][C:8]1[CH:13]=[CH:12][C:11]([CH:14]([CH3:16])[CH3:15])=[CH:10][C:9]=1[N+:17]([O-])=O)([CH3:4])([CH3:3])[CH3:2]>[Pd]>[C:1]([O:5][C:6](=[O:20])[NH:7][C:8]1[CH:13]=[CH:12][C:11]([CH:14]([CH3:15])[CH3:16])=[CH:10][C:9]=1[NH2:17])([CH3:3])([CH3:2])[CH3:4]参加物
3
実験手順
Prepared from (4-isopropyl-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A2) by catalytic hydrogenation with Pd/C according to the general procedure G (method a). Obtained as a white solid (12.59 g).
出典と根拠
- ORDレコード
- ord-4bf12a44d896422692dd442071a39eaf
- 出典データセット
- uspto-grants-2003_01
- 特許番号
- US06509328B1
反応ノート
読み込み中…