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Ammonia → N-(2-t-Butyl-5-carbamoylphenyl)-3-[4-(1-oxobutyl)-2-methoxyphenyl]octanamide

HRID 1637451
ノート
印刷プレビュー

反応式

HRID 1637451 の反応式
[C:1]([C:5]1[CH:10]=[CH:9][C:8]([C:11](O)=[O:12])=[CH:7][C:6]=1[NH:14][C:15](=[O:36])[CH2:16][CH:17]([C:23]1[CH:28]=[CH:27][C:26]([C:29](=[O:33])[CH2:30][CH2:31][CH3:32])=[CH:25][C:24]=1[O:34][CH3:35])[CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])([CH3:4])([CH3:3])[CH3:2].[NH3:37].CCCCCC.C(OCC)(=O)C>C(#N)C>[C:1]([C:5]1[CH:10]=[CH:9][C:8]([C:11](=[O:12])[NH2:37])=[CH:7][C:6]=1[NH:14][C:15](=[O:36])[CH2:16][CH:17]([C:23]1[CH:28]=[CH:27][C:26]([C:29](=[O:33])[CH2:30][CH2:31][CH3:32])=[CH:25][C:24]=1[O:34][CH3:35])[CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])([CH3:4])([CH3:3])[CH3:2]
参加物実験手順後処理出典と根拠反応ノート

参加物

6

反応物 4

HCID 222AmmoniaHCID 8058HexaneHCID 8857Ethyl AcetateHCID 19348698N-(2-t-butyl-5-carboxyphenyl)-3-(4-butyryl-2-methoxyphenyl)octanamide

生成物 1

HCID 19348622N-(2-t-Butyl-5-carbamoylphenyl)-3-[4-(1-oxobutyl)-2-methoxyphenyl]octanamide収率 97%

試薬・触媒・溶媒 1

HCID 6342
Acetonitrile
溶媒

実験手順

210 mg (1.30 mmol) of N,N'-carbonyldiimidazole were added to a suspension of 530 mg (1.07 mmol) of N-(2-t-butyl-5-carboxyphenyl)-3-(4-butyryl-2-methoxyphenyl)octanamide (prepared as described in Preparation 64C), in 10 ml of acetonitrile, and the resulting mixture was stirred for 35 minutes, after which 1.0 ml (15 mmol) of concentrated aqueous ammonia were added. The reaction mixture was stirred for 20 minutes, after which it was freed from the organic solvent by distillation under reduced pressure. The concentrate was extracted with ethyl acetate. The extract was washed with 2 N aqueous hydrochloric acid, with water, with a saturated aqueous solution of sodium hydrogencarbonate and with a saturated aqueous solution of sodium chloride, in that order, after which it was dried over anhydrous magnesium sulfate. The solvent was removed by distillation under reduced pressure, and the resulting residue was purified by column chromatography through 50 g of silica gel using a gradient elution method, with mixtures of hexane and ethyl acetate ranging from 1:9 to 0:9 by volume as the eluent, to give 511 mg (yield 97%) of the title compound as a foam-like substance.

後処理

  1. stirringThe reaction mixture was stirred for 20 minutes
  2. distillationafter which it was freed from the organic solvent by distillation under reduced pressure
  3. extractionThe concentrate was extracted with ethyl acetate
  4. washThe extract was washed with 2 N aqueous hydrochloric acid, with water, with a saturated aqueous solution of sodium hydrogencarbonate and with a saturated aqueous solution of sodium chloride, in that order
  5. dry with materialafter which it was dried over anhydrous magnesium sulfate
  6. customThe solvent was removed by distillation under reduced pressure
  7. customthe resulting residue was purified by column chromatography through 50 g of silica gel using
  8. washa gradient elution method

出典と根拠

ORDレコード
ord-a0955cd9722242408904fba0d29dd448
出典データセット
uspto-grants-2000_03
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US06040339

反応ノート

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