Cyclohexanecarboxylic acid → HCID 22564104、化合物
反応式
[CH:1]1([C:7]([OH:9])=[O:8])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH:10]1(CO)[CH2:15]CCC[CH2:11]1>[Sn]=O.C(O)(C)C>[CH:10]([C:1]1([C:7]([OH:9])=[O:8])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1)([CH3:15])[CH3:11]参加物
5
実験手順
The reaction between cyclohexane carboxylic acid and isopropanol was conducted under the same conditions as in Example 1, except that 1 g of hydrous tin oxide catalyst prepared in Example C was used in place of 2 g of the hydrous zirconium oxide catalyst used in Example 1. It was discovered by gas chromatography that cyclohexyl methanol was formed at a conversion rate of 95% and selectivity of 39%. Isopropyl cyclohexane carboxylic acid was also obtained as a by-product in an amount of 41%.
後処理
- customwas formed at a conversion rate of 95% and selectivity of 39%
出典と根拠
- ORDレコード
- ord-269bf9d0e15d4ae9872659bfd28933c8
- 出典データセット
- uspto-grants-1989_11
- 特許番号
- US04880937
反応ノート
読み込み中…