Sodium Hydroxide → HCID 15096390、化合物

反応式

[OH:1][CH2:2][C:3]([NH:5][CH:6]([C:12]([O:14]CC)=[O:13])[C:7]([O:9]CC)=[O:8])=[O:4].[OH-].[Na+:18]>>[OH:1][CH2:2][C:3]([NH:5][CH:6]([C:12]([O-:14])=[O:13])[C:7]([O-:9])=[O:8])=[O:4].[Na+:18].[Na+:18]

参加物

反応物 2

HCID 14798Sodium Hydroxide

HCID 150963891,3-Diethyl 2-[(2-hydroxyacetyl)amino]propanedioate

生成物 1

HCID 15096390HCID 15096390、化合物

実験手順

Diethyl 2-[(hydroxyacetyl)amino]malonate (0.56 g) is dissolved in 1N aqueous sodium hydroxide (5 ml), and the mixture is reacted at room temperature for 10 hours, and thereafter, the reaction mixture is concentrated under reduced pressure. The residue is washed with methanol to give disodium 2-[(hydroxyacetyl)amino]malonate (0.51 g).

後処理

customthe mixture is reacted at room temperature for 10 hours
concentrationthe reaction mixture is concentrated under reduced pressure
washThe residue is washed with methanol

出典と根拠

ORDレコード: ord-5ecdab6a188f4da69a6a1e8d3cec2ada
出典データセット: uspto-grants-1989_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04882447

反応ノート

読み込み中…

参加物