化工社化工社 化学情報印刷レポート · 研究参考用
Ethambutol Hydrochloride → Ethambutol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethambutol Hydrochloride | HCID 14051 | — |
| 溶媒 | Sodium Carbonate | HCID 10340 | — |
| 溶媒 | Sodium Hydroxide | HCID 14798 | — |
| 生成物 | Ethambutol | HCID 14052 | — |
反応手順
Ethambutol Dihydrochloride (ETB) is obtained from MP Biomedicals (Aurora, Ohio). ETB (7 grams) are dissolved in 100 mL of a saturated solution of sodium carbonate in 5M NaOH. The solution is stirred for 10 minutes and the free based ETB is extracted with three volumes of chloroform. The solution is dried over sodium sulfate. After filtration, the chloroform is removed by rotary evaporation. Ethambutol is represented in the structure below (a).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08119840B2 |
| 出典データセット | uspto-grants-2012_02 |
| ORD ID | ord-bc6a8db3687a4cab96373542461f07a9 |
| 出典メモ | uspto-grants-2012_02 |