HCID 57583245、化合物 → HCID 57583271、化合物
反応式
[CH2:1]([N:8](C)[CH2:9][CH2:10][CH:11]([CH2:24][N:25](CC1C=CC=CC=1)[CH3:26])[CH2:12][CH2:13][CH2:14][N:15](CC1C=CC=CC=1)[CH3:16])C1C=CC=CC=1.[H][H]>[Pd]>[CH3:1][NH:8][CH2:9][CH2:10][CH:11]([CH2:24][NH:25][CH3:26])[CH2:12][CH2:13][CH2:14][NH:15][CH3:16]参加物
4
実験手順
To a methanolic solution of N1,N6-Dibenzyl-3-[(benzyl-methyl-amino)-methyl]-N1,N6-dimethylhexane-1,6-diamine (1 g, 0.002 mol) was added 1 g of Pd/C. The solution was exposed to 2 bar of hydrogen and left to shake for 48 hours at ambient temperature. The reaction mixture was filtered through celite and concentrated at reduced pressure to yield a viscous oil. The structure was confirmed by NMR, yield ˜90%.
後処理
- waitleft
- filtrationThe reaction mixture was filtered through celite
- concentrationconcentrated at reduced pressure
- customto yield a viscous oil
出典と根拠
- ORDレコード
- ord-bfefebd5575f43ba94aafc55c2774683
- 出典データセット
- uspto-grants-2012_02
- 特許番号
- US08124806B2
反応ノート
読み込み中…