Benzyl Alcohol → 2-Benzyltoluene

HRID 1651851

反応式

HRID 1651851 の反応式
[C:1]1([CH3:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:8](O)[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>O>[CH2:7]([C:10]1[CH:11]=[CH:12][CH:13]=[CH:14][C:9]=1[CH3:8])[C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

参加物

4

反応物 2

HCID 244Benzyl Alcohol2 回HCID 1140Toluene

生成物 1

HCID 697382-Benzyltoluene

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

3.170 ml of toluene and 10.5 g of bleaching earth (Tonsil K 10 from Sudchemie AG) were heated to boiling in a stirring vessel with a distillation passage, condenser and water separator. 216 g of benzyl alcohol were then passed in through a jet in the course of about 2 hours, i.e. benzyl alcohol was added dropwise under a flow of nitrogen (100 1/h) via an immersed thin tube and in this way was rapidly and uniformly distributed and made to react.

後処理

  1. additionwas added dropwise under a flow of nitrogen (100 1/h) via an immersed thin tube and in this way
  2. customto react

出典と根拠

ORDレコード
ord-e45e76e1112d4f0ba9561968d73e9ed3
出典データセット
uspto-grants-1990_05
特許番号
US04929784

関連ノート

読み込み中…