Cyclopentene → Dichlorodicyclopentylsilane
反応式
[CH:1]1[CH2:5][CH2:4][CH2:3][CH:2]=1.[Cl:6][SiH2:7][Cl:8]>>[CH:1]1([Si:7]([CH:1]2[CH2:5][CH2:4][CH2:3][CH2:2]2)([Cl:8])[Cl:6])[CH2:5][CH2:4][CH2:3][CH2:2]1参加物
3
実験手順
Cyclopentene in an amount of 136 g (2.00 moles) was made to react with dichlorosilane under various conditions set forth in Table 1, and then the solvent was distilled away. Thus, in analogy with Example 1, dicyclopentyldichlorosilane having a boiling point of 104° C./5 mmHg was obtained in various yields. The yield attained under each reaction condition is shown in Table 1.
後処理
- distillationthe solvent was distilled away
出典と根拠
- ORDレコード
- ord-70339c750cdd4f40bfd6a2d3452b066b
- 出典データセット
- uspto-grants-1995_04
- 特許番号
- US05403947
反応ノート
読み込み中…