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2-Chlorobenzimidazole → Hydrochloric Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Chlorobenzimidazole | HCID 78572 | — |
| 反応物 | 1-Aminotetralin, (R)- | HCID 7058072 | — |
| 生成物 | Hydrochloric Acid | HCID 313 | — |
| 生成物 | NS-8593 | HCID 11587013 | — |
反応手順
The title compound was prepared from 2-chlorobenzimidazole and (R)-1,2,3,4-tetrahydro-l-naphthylamine by Procedure A (40 min at 170° C.). The product was filtered off and washed with acetonitrile to give the title compound as a HCl salt (white solid, mp 264-265° C.). MS(ES+) m/z 264 ([M+1]30, 100).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07737167B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-20c8ebbf2dee4f958242e04dc6a1c9cc |
| 出典メモ | uspto-grants-2010_06 |