HRID16556

反应详情

EQUATION

反应方程式

HRID 16556 的结构方程式

PROCEDURE

实验过程

The title compound was prepared from 2-chlorobenzimidazole and (R)-1,2,3,4-tetrahydro-l-naphthylamine by Procedure A (40 min at 170° C.). The product was filtered off and washed with acetonitrile to give the title compound as a HCl salt (white solid, mp 264-265° C.). MS(ES+) m/z 264 ([M+1]30, 100).

WORKUP

后处理

  1. filtrationThe product was filtered off
  2. washwashed with acetonitrile