Methylamine → HCID 70636802、化合物
反応式
O=[C:2]1[CH2:20][CH2:19][N:5]2[C:6]3[CH:18]=[CH:17][CH:16]=[CH:15][C:7]=3[CH2:8][C:9]3[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=3[CH:4]2[CH2:3]1.[CH3:21][NH2:22].[H][H]>C(O)C.[Pd]>[CH3:21][NH:22][CH:2]1[CH2:20][CH2:19][N:5]2[C:6]3[CH:18]=[CH:17][CH:16]=[CH:15][C:7]=3[CH2:8][C:9]3[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=3[CH:4]2[CH2:3]1参加物
6
実験手順
1 g of 2-keto-1,2,3,4,10,14b-hexahydro-pyridino[1,2-a]-dibenzo[c,f]-azepine is dissolved in 100 ml of ethanol, after which 10 ml of methylamine and 200 mg of palladium (10%) on charcoal are added. Then hydrogen is passed through this mixture until no hydrogen is absorbed any longer.
後処理
- customis absorbed any longer
出典と根拠
- ORDレコード
- ord-640268115d3a4cf9b77a168aedc6fda3
- 出典データセット
- uspto-grants-1976_06
- 特許番号
- US03966723
反応ノート
読み込み中…