Dimethyl Sulfate → HCID 12807407、化合物
反応式
[N+:1]([C:4]1[CH:9]=[C:8]([N+:10]([O-:12])=[O:11])[CH:7]=[C:6]([C:13]([F:16])([F:15])[F:14])[C:5]=1[NH:17][C:18]1[CH:23]=[CH:22][C:21]([O:24][C:25]([F:30])([F:29])[CH:26]([F:28])[F:27])=[CH:20][CH:19]=1)([O-:3])=[O:2].S(OC)(O[CH3:35])(=O)=O.C(=O)([O-])[O-].[Na+].[Na+]>CC(C)=O>[N+:1]([C:4]1[CH:9]=[C:8]([N+:10]([O-:12])=[O:11])[CH:7]=[C:6]([C:13]([F:16])([F:15])[F:14])[C:5]=1[N:17]([CH3:35])[C:18]1[CH:23]=[CH:22][C:21]([O:24][C:25]([F:29])([F:30])[CH:26]([F:28])[F:27])=[CH:20][CH:19]=1)([O-:3])=[O:2]参加物
5
実験手順
Following the procedure of Example 18, N-(2,4-dinitro-6-trifluoromethylphenyl)-4-(1,1,2,2-tetrafluoroethoxy)benzenamine was reacted with dimethyl sulfate and sodium carbonate in acetone to provide N-(2,4-dinitro-6-trifluoromethylphenyl)-N-methyl-4-(1,1,2,2-tetrafluoroethoxy)benzenamine.