1,12-Dichlorododecane → Sodium Hydroxide

反応式

[CH2:1]([C:3]1[CH:9]=[CH:8][C:6]([O-:7])=[CH:5][CH:4]=1)[CH3:2].[Na+:10].Cl[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23]Cl>>[CH2:1]([C:3]1[CH:9]=[CH:8][C:6]([O:7][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][O:7][C:6]2[CH:8]=[CH:9][C:3]([CH2:1][CH3:2])=[CH:4][CH:5]=2)=[CH:5][CH:4]=1)[CH3:2].[OH-:7].[Na+:10]

参加物

反応物 2

HCID 775231,12-Dichlorododecane

HCID 23672322Sodium p-ethylphenolate

生成物 2

HCID 14798Sodium Hydroxide

HCID 53795930HCID 53795930、化合物

実験手順

1,12-bis (4-ethylphenoxy) dodecane is prepared from sodium 4-ethylphenoxide and 1,12-dichlorododecane, according to the method of Example 1, and sulfonated to the disulfonic acid derivative and neutralized with sodium hydroxide according to the method of Example 2, to afford the disodium sulfonate derivative.

出典と根拠

ORDレコード: ord-08439230fa134c5e9c08f0a63023873c
出典データセット: uspto-grants-1981_12
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04307078

反応ノート

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