Hydrochloric Acid → HCID 54392493、化合物

HRID 1660541ノート

反応式

HRID 1660541 の反応式
[CH2:1]([C:4]1[CH:5]=[C:6]([C:11]([C:14]2[CH:19]=[CH:18][C:17]([OH:20])=[C:16]([CH2:21][CH:22]=[CH2:23])[CH:15]=2)([CH3:13])[CH3:12])[CH:7]=[CH:8][C:9]=1[OH:10])[CH:2]=[CH2:3].[OH-].[K+].Cl>>[CH:21]([C:16]1[CH:15]=[C:14]([C:11]([C:6]2[CH:7]=[CH:8][C:9]([OH:10])=[C:4]([CH:1]=[CH:2][CH3:3])[CH:5]=2)([CH3:12])[CH3:13])[CH:19]=[CH:18][C:17]=1[OH:20])=[CH:22][CH3:23]

参加物

4

反応物 3

HCID 313Hydrochloric AcidHCID 14797Potassium HydroxideHCID 74457Phenol, 4,4'-(1-methylethylidene)bis(2-(2-propen-1-yl)-

生成物 1

HCID 54392493HCID 54392493、化合物

実験手順

2,2-Bis(3-allyl-4-hydroxyphenyl)propane (1 mole) was mixed with potassium hydroxide pellets (2.2 moles) and the mixture was stirred and heated at 110° for 30 minutes. The mixture was cooled, neutralised with dilute hydrochloric acid, and the product was extracted to give methylene chloride. The solution was dried and evaporated to give substantially pure 2,2-bis(3-(1-propenyl)-4-hydroxyphenyl)propane.

後処理

  1. temperatureheated at 110° for 30 minutes
  2. temperatureThe mixture was cooled
  3. extractionthe product was extracted
  4. customto give methylene chloride
  5. customThe solution was dried
  6. customevaporated

出典と根拠

ORDレコード
ord-e483e07df4414dc0bf7f15894c8d1bb4
出典データセット
uspto-grants-1981_12
特許番号
US04308367

反応ノート

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