Nitric Acid → Norvaline Dinitrate

HRID 1663212

反応式

HRID 1663212 の反応式
[N+:1]([O-:4])([OH:3])=[O:2].[NH2:5][C@H:6]([C:10]([OH:12])=[O:11])[CH2:7][CH2:8][CH3:9].[N+:13]([O-:16])([OH:15])=[O:14].[NH2:17][C@H:18]([C:22]([OH:24])=[O:23])[CH2:19][CH2:20][CH3:21]>O>[N+:1]([O-:4])([OH:3])=[O:2].[N+:13]([O-:16])([OH:15])=[O:14].[NH2:5][C@H:6]([C:10]([OH:12])=[O:11])[CH2:7][CH2:8][CH3:9].[N+:1]([O-:4])([OH:3])=[O:2].[N+:1]([O-:4])([OH:3])=[O:2].[N+:1]([O-:4])([OH:3])=[O:2].[NH2:17][C@H:18]([C:22]([OH:24])=[O:23])[CH2:19][CH2:20][CH3:21]

参加物

6

反応物 3

HCID 944Nitric AcidHCID 65098L-NorvalineHCID 86628854HCID 86628854、化合物

生成物 2

HCID 86628852Norvaline DinitrateHCID 86628853Norvaline Trinitrate

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Applicants have cost-effectively synthesized Norvaline Nitrate by combining nitric acid and Norvaline, mixing with water, and leaving to crystallize. Further nitratization can take place, yielding Norvaline Dinitrate or Norvaline Trinitrate. An alternative implementation comprises substituting Nitrous Acid (HNO2) for Nitric Acid (HNO3), thus yielding Norvaline Nitrite. Norvaline Nitrite has the same effects as Norvaline Nitrate, the only difference being that it requires one less step to yield Nitric Oxide (NO—). Mixed salts may also be used, such as in the non-limiting example of Norvaline Nitrate-Orotate.

後処理

  1. customleaving
  2. customto crystallize

出典と根拠

ORDレコード
ord-1e202537f69a4623a9e929cd9675d280
出典データセット
uspto-grants-2011_10
特許番号
US08034836B2

関連ノート

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