Nitric Acid → 3-Bromo-4-hydroxy-5-nitrobenzaldehyde

HRID 1663361ノート

反応式

HRID 1663361 の反応式
[Br:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][C:9]=1[OH:10])[CH:5]=[O:6].[N+:11]([O-])([OH:13])=[O:12]>C(O)(=O)C>[Br:1][C:2]1[CH:3]=[C:4]([CH:7]=[C:8]([N+:11]([O-:13])=[O:12])[C:9]=1[OH:10])[CH:5]=[O:6]

参加物

4

反応物 2

HCID 944Nitric AcidHCID 763083-Bromo-4-hydroxybenzaldehyde

生成物 1

HCID 14943783-Bromo-4-hydroxy-5-nitrobenzaldehyde

試薬・触媒・溶媒 1

HCID 176Acetic Acid溶媒

実験手順

3-Bromo-4-hydroxybenzaldehyde (250 mg) was dissolved in 5 ml of acetic acid. Nitric acid (52 μl) was added and the mixture was stirred for 3 h during which a solid formed. The solid was filtered off, washed with water and dried in vacuo.

後処理

  1. customformed
  2. filtrationThe solid was filtered off
  3. washwashed with water
  4. customdried in vacuo

出典と根拠

ORDレコード
ord-1f5b60dd7fee4c75b87a95ec00faca54
出典データセット
uspto-grants-2011_10
特許番号
US08034945B2

反応ノート

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