Sodium Hydroxide → 4-Azidobutanoic Acid
反応式
[N:1]([CH2:4][CH2:5][CH2:6][C:7]([O:9]C)=[O:8])=[N+:2]=[N-:3].[OH-].[Na+]>CO>[N:1]([CH2:4][CH2:5][CH2:6][C:7]([OH:9])=[O:8])=[N+:2]=[N-:3]参加物
4
実験手順
Methyl 4-azidobutanoate was suspended in 1N NaOH (1.2 eq) and the minimum of MeOH was added to make the reaction mixture homogenous. After 1 h at RT temperature, MeOH was removed in vacuo. The aqueous solution
後処理
- customAfter 1 h at RT temperature, MeOH was removed in vacuo
出典と根拠
- ORDレコード
- ord-addf8ec2b522498fb66858206aa8654e
- 出典データセット
- uspto-grants-2011_08
- 特許番号
- US07989438B2
反応ノート
読み込み中…