Thionyl Chloride → 1-Methyl-cycloheptanecarbonyl chloride
反応式
[CH3:1][C:2]1([C:9]([OH:11])=O)[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1.S(Cl)([Cl:14])=O>>[CH3:1][C:2]1([C:9]([Cl:14])=[O:11])[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1参加物
3
実験手順
A solution of 1-methyl-cycloheptanecarboxylic acid (156 mg, 0.998 mmol) (Journal of Organic Chemistry (1982), 47(17), 3242-7) in thionyl chloride (5 ml) was stirred at room temperature for 2 days and then concentrated on high vacuum giving 174 mg (99%) of 1-methyl-cycloheptanecarbonyl chloride as a yellow oil.
後処理
- concentrationconcentrated on high vacuum
出典と根拠
- ORDレコード
- ord-43cd66044f5f4b11b68e96d62e7621d2
- 出典データセット
- uspto-grants-2011_08
- 特許番号
- US08008298B2
反応ノート
読み込み中…