(+-)-4-Methylhexanoic acid → HCID 12600624、化合物

反応式

[CH3:1][CH:2]([CH2:8][CH3:9])[CH2:3][CH2:4][C:5](O)=[O:6].S(Cl)([Cl:12])=O>>[CH3:1][CH:2]([CH2:8][CH3:9])[CH2:3][CH2:4][C:5]([Cl:12])=[O:6]

参加物

反応物 2

HCID 15271(+-)-4-Methylhexanoic acid

HCID 24386Thionyl Chloride

生成物 1

HCID 12600624HCID 12600624、化合物

実験手順

The acid from step A2 is converted into the acid chloride by interaction with thionyl chloride according to a standard method. After removal of the excess of thionyl chloride, the residual acid chloride is used in step C2 without further purification.

後処理

customAfter removal of the excess of thionyl chloride
customthe residual acid chloride is used in step C2 without further purification

出典と根拠

ORDレコード: ord-677e682bdd7c48c3b1e43681e0ff2d2d
出典データセット: uspto-grants-1978_03
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04077260

反応ノート

読み込み中…

参加物