Water → 4-(Naphthalen-1-yloxy)aniline
反応式
O.[C:2]1([O:12][C:13]2[CH:18]=[CH:17][C:16]([N+:19]([O-])=O)=[CH:15][CH:14]=2)[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][CH:3]=1>[Fe].C(O)(=O)C>[C:2]1([O:12][C:13]2[CH:18]=[CH:17][C:16]([NH2:19])=[CH:15][CH:14]=2)[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][CH:3]=1参加物
5
実験手順
A mixture of 1.5 liters of water, 40 ml of glacial acetic acid and 1.0 mol of 4-(α-naphthoxy)-nitrobenzene was heated to boiling while stirring. After the boiling temperature had been reached, 200 g of iron powder were added in small portions. When the addition was finished, it was refluxed for 6 hours, while stirring.
後処理
- temperaturewas heated
- additionWhen the addition
- temperatureit was refluxed for 6 hours
- stirringwhile stirring
出典と根拠
- ORDレコード
- ord-645f2b93eea24ca7bb3c17dc790bef29
- 出典データセット
- uspto-grants-1981_06
- 特許番号
- US04275077
反応ノート
読み込み中…