Nitric Acid → 2,4-Dichloro-3-nitrobenzoic acid

HRID 1682150ノート

反応式

HRID 1682150 の反応式
[N+:1]([O-:4])(O)=[O:2].[Cl:5][C:6]1[CH:14]=[C:13]([Cl:15])[CH:12]=[CH:11][C:7]=1[C:8]([OH:10])=[O:9]>S(=O)(=O)(O)O>[Cl:5][C:6]1[C:14]([N+:1]([O-:4])=[O:2])=[C:13]([Cl:15])[CH:12]=[CH:11][C:7]=1[C:8]([OH:10])=[O:9]

参加物

4

反応物 2

HCID 944Nitric AcidHCID 57872,4-Dichlorobenzoic Acid

生成物 1

HCID 190232292,4-Dichloro-3-nitrobenzoic acid

試薬・触媒・溶媒 1

HCID 1118Sulfuric Acid溶媒

実験手順

To a solution of 25 ml of fuming nitric acid and 20 ml of sulfuric acid, 25 g of 2,4-dichlorobenzoic acid was gradually added. After completion of the heat generation, the reaction mixture was poured into ice water. Precipitated solid was washed with water and dried to obtain 23.0 g of the desired product.

後処理

  1. customPrecipitated solid
  2. washwas washed with water
  3. customdried

出典と根拠

ORDレコード
ord-e8fb074dc0314d3da49e00c91f786941
出典データセット
uspto-grants-1992_12
特許番号
US05175299

反応ノート

読み込み中…