Methylamine → HCID 67264048、化合物
反応式
[N+:1]([C:4]1[CH:15]=[CH:14][C:7]2[C:8](=[O:13])OC(=O)[NH:11][C:6]=2[CH:5]=1)([O-:3])=[O:2].[CH3:16][NH2:17]>C1COCC1>[NH2:11][C:6]1[CH:5]=[C:4]([N+:1]([O-:3])=[O:2])[CH:15]=[CH:14][C:7]=1[C:8]([NH:17][CH3:16])=[O:13]参加物
4
実験手順
7-Nitro-1H-3,1-benzoxazine-2,4-dione (1.14 g, 0.00549 mol) was dissolved in THF (50 mL, 0.6 mol). 2 M of Methylamine in THF (10 mL) was added, and a yellow solid formed immediately. The reaction mixture was concentrated under reduced pressure to afford a light orange solid.
後処理
- customa yellow solid formed immediately
- concentrationThe reaction mixture was concentrated under reduced pressure
- customto afford a light orange solid
出典と根拠
- ORDレコード
- ord-5490aeb9ffa549e19adc97176d7f67f3
- 出典データセット
- uspto-grants-2012_04
- 特許番号
- US08148391B2
反応ノート
読み込み中…