Dimethylamine → 5-(Dimethylamino)-2-nitrobenzoic acid
反応式
Cl[C:2]1[CH:3]=[CH:4][C:5]([N+:11]([O-:13])=[O:12])=[C:6]([CH:10]=1)[C:7]([OH:9])=[O:8].[CH3:14][NH:15][CH3:16]>>[CH3:14][N:15]([CH3:16])[C:2]1[CH:3]=[CH:4][C:5]([N+:11]([O-:13])=[O:12])=[C:6]([CH:10]=1)[C:7]([OH:9])=[O:8]参加物
3
実験手順
Concretely, 5-chloro-2-nitrobenzoic acid is dissolved in a dimethylamine aqueous solution and heated to produce 5-dimethylamino-2-nitrobenzoic acid. Hydrochloric acid is added to the reaction solution to precipitate out the product as a solid material. The solid material is separated to obtain 5-dimethylamno-2-nitrobenzoic acid almost quantitatively.
後処理
- temperatureheated
出典と根拠
- ORDレコード
- ord-d83951711c72435a9bf755e0eb273d0b
- 出典データセット
- uspto-grants-2010_06
- 特許番号
- US07737274B2
反応ノート
読み込み中…