関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 1,3-Diiodopropane | HCID 12314 | — |
| 反応物 | 3-Methyl-6-methylthiopurine | HCID 248868 | — |
| 生成物 | HCID 178503588 | HCID 178503588 | 28% |
反応手順
A pressure tube, equipped with a magnetic stirring bar, was charged with Compound 2 (0.54 g, 3 mmole) and 1,3-diiodopropane (2.66 g, 9 mmole). The mixture was heated to ˜120° C. for 3 hours. The residue was extensively washed with ethyl acetate and diethyl ether and dried under vacuum to give 0.4 g of yellow solid Compound 3 (yield ˜28%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07737281B2 |
|---|
| 出典データセット | uspto-grants-2010_06 |
|---|
| ORD ID | ord-462658577d844d109c373b1b32a7fd9e |
|---|
| 出典メモ | uspto-grants-2010_06 |
|---|
