関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2-Butanamine, 2-methyl- | HCID 68986 | — |
| 反応物 | 2-Isothiocyanato-1,3-bis(propan-2-yl)benzene | HCID 141194 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | N-(2,6-Diisopropyl-phenyl)-N'-tert.-pentyl-thiourea | HCID 20347005 | — |
反応手順
11.0 g of 2,6-diisopropyl-phenyl isothiocyanate and 10 g of tert.-pentylamine are warmed with 5 ml of triethylamine for 10 minutes at 100°. After standing for 12 hours, the mixture which has partially crystallised out is stirred with petroleum ether and cooled to -10° C., and the product is filtered off and dried.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04194008 |
|---|
| 出典データセット | uspto-grants-1980_03 |
|---|
| ORD ID | ord-d9b862f4e5314eeca858816b39825fce |
|---|
| 出典メモ | uspto-grants-1980_03 |
|---|
