反应详情

温度

-10 °C

11.0 g of 2,6-diisopropyl-phenyl isothiocyanate and 10 g of tert.-pentylamine are warmed with 5 ml of triethylamine for 10 minutes at 100°. After standing for 12 hours, the mixture which has partially crystallised out is stirred with petroleum ether and cooled to -10° C., and the product is filtered off and dried.

1. customthe mixture which has partially crystallised out
2. filtrationthe product is filtered off
3. customdried