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Sodium hydride → 7-(3-Ethyl-4.5-diphenyl-2-oxo-4-imidazolin-1-yl) enanthic acid ethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium hydride | HCID 24758 | — |
| 反応物 | Ethyl 7-chloroheptanoate | HCID 529988 | — |
| 反応物 | 1-ethyl-4,5-diphenyl-1,3-dihydro-2H-imidazol-2-one | HCID 12675126 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | 7-(3-Ethyl-4.5-diphenyl-2-oxo-4-imidazolin-1-yl) enanthic acid ethyl ester | HCID 53708715 | — |
反応手順
The product is obtained as described in example 1 from 2.1 g of NaH (80% suspension in mineral oil), 18.5 g of 1-ethyl-4.5-diphenyl-4-imidazolin-2-one, 140 cc. of DMF, 13.5 g of 7-chloroenanthic acid ethyl ester and 2.1 g of NaJ.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04349684 |
| 出典データセット | uspto-grants-1982_09 |
| ORD ID | ord-5c9d7533d6a6403cad679228344b1a0a |
| 出典メモ | uspto-grants-1982_09 |