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Sodium hydride → 8-[3-(4-Chlorophenyl)-2-oxo-4-phenyl-4-imidazolin-1-yl] caprylic acid methyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium hydride | HCID 24758 | — |
| 反応物 | Methyl 8-bromooctanoate | HCID 11107373 | — |
| 反応物 | 1-(4-Chlorophenyl)-5-phenyl-4-imidazolin-2-one | HCID 12418988 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | 8-[3-(4-Chlorophenyl)-2-oxo-4-phenyl-4-imidazolin-1-yl] caprylic acid methyl ester | HCID 53727203 | — |
反応手順
The product is produced as described in example 1 from 2.4 g of NaH (80% suspension in mineral oil), 21.6 g of 1-(4-chlorophenyl)-5-phenyl-4-imidazolin-2-one, 160 cc. of DMF, 19.0 g of 8-bromocaprylic acid methyl ester and 2.4 g of NaJ.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04349684 |
| 出典データセット | uspto-grants-1982_09 |
| ORD ID | ord-7c3f831edb2f4b4290cd9e8903598d1d |
| 出典メモ | uspto-grants-1982_09 |