Magnesium Hydroxide → 2-Hydroxyimino-2-(1,2,5-thiadiazol-3-yl)acetic acid
反応式
[S:1]1[N:5]=[CH:4][C:3]([C:6](=O)[C:7]([OH:9])=[O:8])=[N:2]1.Cl.[NH2:12][OH:13].[OH-].[Mg+2].[OH-]>>[OH:13][N:12]=[C:6]([C:3]1[CH:4]=[N:5][S:1][N:2]=1)[C:7]([OH:9])=[O:8]参加物
4
実験手順
2-(1,2,5-Thiadiazol-3-yl)glyoxylic acid (7.4 g.) and hydroxylamine hydrochloride (3.1 g.) were reacted in the presence of magnesium hydroxide (4.7 g.) according to a similar manner to that of Example 6(a)(3) to give 2-hydroxyimino-2-(1,2,5-thiadiazol-3-yl)acetic acid (syn isomer) (7.5 g.).
出典と根拠
- ORDレコード
- ord-19f602d3d833424894f7beb3f4315ae9
- 出典データセット
- uspto-grants-1982_09
- 特許番号
- US04350693
反応ノート
読み込み中…