Hydrochloric Acid → 5-(Chloromethyl)uracil

HRID 1703050

反応式

HRID 1703050 の反応式
O[CH2:2][C:3]1[C:4](=[O:10])[NH:5][C:6](=[O:9])[NH:7][CH:8]=1.[ClH:11]>>[Cl:11][CH2:2][C:3]1[C:4](=[O:10])[NH:5][C:6](=[O:9])[NH:7][CH:8]=1

参加物

3

実験手順

A solution of 1.4 g. (0.010 mole) of 5-hydroxymethyl uracil in 12.5 ml. of concentrated hydrochloric acid was prepared. A colorless precipitate (5-chloromethyl uracil) formed within two minutes and after about ten minutes the precipitate was collected by filtration, washed rapidly with ice cold water, dried and then suspended in 10 ml. of dimethylformamide.

出典と根拠

ORDレコード
ord-4dcebf16c68b4e21871e38c7da8478f6
出典データセット
uspto-grants-1982_09
特許番号
US04350754

関連ノート

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