Diazomethane → 3'-Sulfamoyl-diazoacetophenone

HRID 1703892

反応式

HRID 1703892 の反応式
[S:1]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][CH:13]=1)[C:8](Cl)=[O:9])(=[O:4])(=[O:3])[NH2:2].[N+:14](=[CH2:16])=[N-:15]>C(OCC)C>[S:1]([C:5]1[CH:6]=[C:7]([C:8](=[O:9])[CH:16]=[N+:14]=[N-:15])[CH:11]=[CH:12][CH:13]=1)(=[O:4])(=[O:3])[NH2:2]

参加物

4

反応物 2

HCID 9550DiazomethaneHCID 188018833-Sulfamoylbenzoyl chloride

生成物 1

HCID 537058143'-Sulfamoyl-diazoacetophenone

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒

実験手順

11 g of 3-sulfamoylbenzoyl chloride were reacted as prescribed in Example 66(b) with diazomethane in diethyl ether and the crystals were filtered off. Melting point: 142° C.

後処理

  1. filtrationthe crystals were filtered off

出典と根拠

ORDレコード
ord-7b76b92ee76248ee9688dd46101d8ddc
出典データセット
uspto-grants-1978_11
特許番号
US04125614

関連ノート

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