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Diazomethane → 3'-Sulfamoyl-diazoacetophenone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diazomethane | HCID 9550 | — |
| 反応物 | 3-Sulfamoylbenzoyl chloride | HCID 18801883 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | 3'-Sulfamoyl-diazoacetophenone | HCID 53705814 | — |
反応手順
11 g of 3-sulfamoylbenzoyl chloride were reacted as prescribed in Example 66(b) with diazomethane in diethyl ether and the crystals were filtered off. Melting point: 142° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04125614 |
| 出典データセット | uspto-grants-1978_11 |
| ORD ID | ord-7b76b92ee76248ee9688dd46101d8ddc |
| 出典メモ | uspto-grants-1978_11 |