反応式
[Cl:1][CH2:2][C:3]([O:5][C:6]1[CH:11]=[CH:10][C:9]([NH:12][C:13](=[O:15])[CH3:14])=[CH:8][CH:7]=1)=[O:4].[CH2:16]([NH:18][CH2:19][CH3:20])[CH3:17].C(N(CC)CC)C>O>[ClH:1].[CH2:16]([N:18]([CH2:2][C:3]([O:5][C:6]1[CH:11]=[CH:10][C:9]([NH:12][C:13](=[O:15])[CH3:14])=[CH:8][CH:7]=1)=[O:4])[CH2:19][CH3:20])[CH3:17]参加物
5
実験手順
22.8 g of p-acetamidophenyl chloroacetate were added in small portions to a solution of 7.5 g of diethylamine in 30 c.c. of triethylamine with stirring, while the temperature was maintained at between 40° C. and 50° C. with a bath of cold water if necessary. The process described in Example 1 was then followed to obtain 12 g of p-acetamidophenyl diethylaminoacetate hydrochloride melting point = 228° C.
出典と根拠
- ORDレコード
- ord-abc1d9f1c5e84e8e9fbe8e110565d271
- 出典データセット
- uspto-grants-1978_11
- 特許番号
- US04127671
関連ノート
読み込み中…