1-Octanol → Dicaprylyl Ether

HRID 1719986

反応式

HRID 1719986 の反応式
[CH2:1]([OH:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S([CH:14]([CH2:18][C:19](O)=O)[C:15](O)=O)(O)(=O)=O>O>[CH2:1]([O:9][CH2:15][CH2:14][CH2:18][CH2:19][CH2:1][CH2:2][CH2:3][CH3:4])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

参加物

4

反応物 2

HCID 9571-OctanolHCID 21220Sulfosuccinic acid monosodium salt

生成物 1

HCID 12399Dicaprylyl Ether

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

206 kg (1581.8 moles) of n-octanol were heated to 190°-210° C. together with 2.94 kg of sulfosuccinic acid (70% by weight). The water of reaction formed was distilled off. After 7 hours, 10.3 g of 50% by weight sodium hydroxide were added to the cooled reaction mixture for neutralization, after which the crude product was washed until neutral and then distilled.

後処理

  1. customformed
  2. distillationwas distilled off
  3. addition10.3 g of 50% by weight sodium hydroxide were added to the cooled reaction mixture for neutralization
  4. washafter which the crude product was washed until neutral and
  5. distillationthen distilled

出典と根拠

ORDレコード
ord-e296b566e6b848bf9c01de3be92734cb
出典データセット
uspto-grants-1996_04
特許番号
US05503760

関連ノート

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