化工社化工社 化学情報印刷レポート · 研究参考用
1-Octanol → Dicaprylyl Ether
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Octanol | HCID 957 | — |
| 反応物 | Sulfosuccinic acid monosodium salt | HCID 21220 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Dicaprylyl Ether | HCID 12399 | — |
反応手順
206 kg (1581.8 moles) of n-octanol were heated to 190°-210° C. together with 2.94 kg of sulfosuccinic acid (70% by weight). The water of reaction formed was distilled off. After 7 hours, 10.3 g of 50% by weight sodium hydroxide were added to the cooled reaction mixture for neutralization, after which the crude product was washed until neutral and then distilled.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05503760 |
| 出典データセット | uspto-grants-1996_04 |
| ORD ID | ord-e296b566e6b848bf9c01de3be92734cb |
| 出典メモ | uspto-grants-1996_04 |