反应详情

206 kg (1581.8 moles) of n-octanol were heated to 190°-210° C. together with 2.94 kg of sulfosuccinic acid (70% by weight). The water of reaction formed was distilled off. After 7 hours, 10.3 g of 50% by weight sodium hydroxide were added to the cooled reaction mixture for neutralization, after which the crude product was washed until neutral and then distilled.

1. customformed
2. distillationwas distilled off
3. addition10.3 g of 50% by weight sodium hydroxide were added to the cooled reaction mixture for neutralization
4. washafter which the crude product was washed until neutral and
5. distillationthen distilled