Ethanol → HCID 20070367、化合物
反応式
[CH3:1][C:2]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[N+:13]([O-])=O)([CH3:5])[CH2:3][OH:4].[CH2:16](O)[CH3:17]>[Pd]>[CH3:16][C:17]1[N:6]([C:2]([CH3:5])([CH3:1])[CH2:3][OH:4])[C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=2[N:13]=1参加物
4
実験手順
2-(1,1-dimethyl-2-hydroxyethyl)aminonitrobenzene (10 g) in ethanol (200 ml) was hydrogenated at 50 p.s.i. (345 kPa) over 5% Pd/C (0.5 g) for 2 hours. The catalyst was filtered off and the solvent removed under reduced pressure yielding the title compound as a yellow foam 8.4 g (98%).
後処理
- filtrationThe catalyst was filtered off
- customthe solvent removed under reduced pressure
出典と根拠
- ORDレコード
- ord-b46d2edbc7134b9ea6451dda46bf3440
- 出典データセット
- uspto-grants-1989_08
- 特許番号
- US04853392
反応ノート
読み込み中…