Triethylamine → N,N'-bis(allyl)carbodiimide
反応式
[CH2:1]([NH:4][C:5]([NH:7][CH2:8][CH:9]=[CH2:10])=S)[CH:2]=[CH2:3].C(N(CC)CC)C.[I-].ClC1C=CC=C[N+]=1C>C(#N)C>[CH2:1]([N:4]=[C:5]=[N:7][CH2:8][CH:9]=[CH2:10])[CH:2]=[CH2:3]参加物
5
実験手順
1.56 g of N,N'-bis(allyl)thiourea, 2.4 g of triethylamine and 3.07 g of 2-chloro-1-methylpyridinium iodide are reacted in 40 ml of acetonitrile and the reaction mixture is worked up as described in Example 4. The product is obtained as a faintly yellowish oil.
後処理
- customThe product is obtained as a faintly yellowish oil
出典と根拠
- ORDレコード
- ord-b1e719b11ff545e7ba7de4d2f9e2dd6e
- 出典データセット
- uspto-grants-1989_08
- 特許番号
- US04859761
反応ノート
読み込み中…