Thionyl Chloride → HCID 20025664、化合物

HRID 1723408ノート

反応式

HRID 1723408 の反応式
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][C:17]([OH:19])=O)=[CH:5][CH:4]=1.S(Cl)([Cl:22])=O>C(Cl)Cl>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][C:17]([Cl:22])=[O:19])=[CH:5][CH:4]=1

参加物

4

反応物 2

HCID 24386Thionyl ChlorideHCID 14555669HCID 14555669、化合物

生成物 1

HCID 20025664HCID 20025664、化合物

試薬・触媒・溶媒 1

HCID 6344Dichloromethane溶媒

実験手順

To an ice-cold, stirring solution of 3 gm 9(4-methoxyphenyl)nonanoic acid in 10 ml. CH2Cl2 was added dropwise 1.2 ml thionyl chloride. The solution was then allowed to warm up to room temperature. The solvent and excess thionyl chloride were removed in vacuo to give a brown oil, which was used directly in the last step without further purification.

後処理

  1. customThe solvent and excess thionyl chloride were removed in vacuo
  2. customto give a brown oil, which
  3. customwas used directly in the last step without further purification

出典と根拠

ORDレコード
ord-aab12e7043bc497c8d1a1db10757b098
出典データセット
uspto-grants-1989_08
特許番号
US04861798

反応ノート

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