1-Phenylcyclohexane-1-carboxylic acid → Methyl 1-phenylcyclohexane-1-carboxylate

HRID 1729067

反応式

HRID 1729067 の反応式
[C:1]1([C:7]2([C:13]([OH:15])=[O:14])[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:16]OC(C1CCCC1)=O>CCOCC>[CH3:16][O:14][C:13]([C:7]1([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8]1)=[O:15]

参加物

4

反応物 2

HCID 708171-Phenylcyclohexane-1-carboxylic acidHCID 78365Methyl cyclopentanecarboxylate

生成物 1

HCID 15105202Methyl 1-phenylcyclohexane-1-carboxylate

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒

実験手順

This compound was prepared (1.91 g, 8.76 mmol, 89%) from the product of Step A (2.00 g, 9.8 mmol) following the procedure for synthesis of methyl-1-cyclopentanecarboxylate as set forth in Step A, Example 1. The product of this step was homogeneous by TLC (ether:C2Cl2, 2:1) and used in the next step without further purification. CIMS 219 m/z (M+1).

後処理

  1. customused in the next step without further purification

出典と根拠

ORDレコード
ord-a3d1cba68a344dc4abd002d70273a898
出典データセット
uspto-grants-1994_07
特許番号
US05331010

関連ノート

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