Ethylamine → 4-Ethylamino-3-nitrobenzamide

HRID 1729581

反応式

HRID 1729581 の反応式
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1Cl)[C:7]([NH2:9])=[O:8])([O-:3])=[O:2].[CH2:14]([NH2:16])[CH3:15]>>[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[NH:16][CH2:14][CH3:15])[C:7]([NH2:9])=[O:8])([O-:3])=[O:2]

参加物

3

反応物 2

HCID 6341EthylamineHCID 279424-Chloro-3-nitrobenzamide

生成物 1

HCID 37089224-Ethylamino-3-nitrobenzamide

実験手順

II (160 g - 0.8 mole) was added portionwise with stirring at 60° C to 720 g of 50 % by weight aqueous ethylamine. The mixture was cooled, the precipitate was collected and crystallized from the monomethyl ether of ethylene glycol (5 ml per gram of dried product).

後処理

  1. temperatureThe mixture was cooled
  2. customthe precipitate was collected
  3. customcrystallized from the monomethyl ether of ethylene glycol (5 ml per gram of dried product)

出典と根拠

ORDレコード
ord-bb3097a7e15a44488e01fcb467723d81
出典データセット
uspto-grants-1976_11
特許番号
US03989522

関連ノート

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