Methanol → HCID 13878920、化合物
反応式
C([NH:11][CH:12]([CH3:24])[CH2:13][O:14][CH:15]1[CH:19]([CH3:20])[CH2:18][CH:17](C)[C:16]1([CH3:23])[CH3:22])(OCC1C=CC=CC=1)=O.[CH3:25]O>[Pd]>[NH2:11][CH:12]([CH3:24])[CH2:13][O:14][CH:15]1[C:16]([CH3:22])([CH3:23])[CH2:17][CH2:18][C:19]1([CH3:20])[CH3:25]参加物
4
実験手順
N-Cbz-1-(2-Aminopropoxy)-2,2,3,5-tetramethylcyclopentane is dissolved in CH3OH and hydrogenated over 5% Pd/C in a Parr hydrogenation apparatus. When the reaction is complete the mixture is filtered through Celite and concentrated to yield 1-(2-amino-propoxy)-2,2,5,5-tetramethylcyclopentane.
後処理
- filtrationis filtered through Celite
- concentrationconcentrated
出典と根拠
- ORDレコード
- ord-a5d949f8b797490281f9bc314fda3f5e
- 出典データセット
- uspto-grants-1986_11
- 特許番号
- US04622418
反応ノート
読み込み中…