反応式
[C:1]([CH2:3][NH:4][C:5]([NH2:7])=[O:6])#[N:2].[OH-:8].[Na+].[CH3:10]O>>[CH3:10][O:8][C:1](=[NH:2])[CH2:3][NH:4][C:5]([NH2:7])=[O:6]参加物
4
反応条件
- 温度
- 20 °C
実験手順
100 g of cyanomethylurea is combined with a mixture of 300 ml of methanol and 5 ml of 8N sodium hydroxide solution and stirred for 3 hours at 25°-30° C. The mixture is allowed to cool to 20° C., the resultant product is removed by filtration, washed with a small amount of ice-cold methanol, and dried under vacuum, thus obtaining 92.6 g of (2-methoxy-2-iminoethyl)urea (=70% of theory).
後処理
- customthe resultant product is removed by filtration
- washwashed with a small amount of ice-cold methanol
- customdried under vacuum
出典と根拠
- ORDレコード
- ord-71e78e38058f4f998cc71a26bcecb38b
- 出典データセット
- uspto-grants-1986_11
- 特許番号
- US04623730
関連ノート
読み込み中…