反応式
[NH2:1][C:2]1[CH:7]=[CH:6][N:5]=[CH:4][CH:3]=1.S(=O)(=O)(O)O.[N+:13]([O-])([OH:15])=[O:14].NC1C([N+]([O-])=O)=NC=CC=1.NC(C)C#N>>[NH2:1][C:2]1[CH:7]=[CH:6][N:5]=[CH:4][C:3]=1[N+:13]([O-:15])=[O:14]参加物
6
実験手順
4-Amino-3-nitropyridine was synthesized by a literature reference [Harris M. G. and Stewart R. Can. J. Chem. 55, 3800 (1977)]; by nitration of 4-aminopyridine with conc. sulfuric acid and fuming nitric acid. This aminonitropyridine was then converted to the aminopropionitrile derivative IV by the method described in Example 1.
出典と根拠
- ORDレコード
- ord-43f197b3e3d046e6af821251aff2b1c6
- 出典データセット
- uspto-grants-1999_10
- 特許番号
- US05968946
関連ノート
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