Thionyl Chloride → HCID 54108381、化合物
反応式
[CH:1]([C:4]1[CH:11]=[CH:10][CH:9]=[C:8]([CH:12]([CH3:14])[CH3:13])[C:5]=1[CH2:6]O)([CH3:3])[CH3:2].S(Cl)([Cl:17])=O>C1(C)C=CC=CC=1>[CH:1]([C:4]1[CH:11]=[CH:10][CH:9]=[C:8]([CH:12]([CH3:14])[CH3:13])[C:5]=1[CH2:6][Cl:17])([CH3:3])[CH3:2]参加物
4
実験手順
To a solution of 1.37 g (7.12 mmol) of 2, 6-diisopropylbenzyl alcohol in 20 ml of toluene was added 0.78 ml (10.7 mmol) of thionyl chloride, and the resultant mixture was stirred at room temperature for 3.5 hours. The reaction mixture was washed with water, dried over anhydrous magnesium sulfate and the solvent evaporated in vacuo to give 1.49 g of 2, 6-diisopropylbenzyl chloride as an oil.
後処理
- washThe reaction mixture was washed with water
- dry with materialdried over anhydrous magnesium sulfate
- customthe solvent evaporated in vacuo
出典と根拠
- ORDレコード
- ord-23c7f3a620a7481f9b504a21409aa50a
- 出典データセット
- uspto-grants-1995_08
- 特許番号
- US05442060
反応ノート
読み込み中…