Sulfamide → HCID 178479209、化合物

HRID 1762977

反応式

HRID 1762977 の反応式
[S:1]([NH2:5])([NH2:4])(=[O:3])=[O:2].Cl.[Cl:7][CH2:8][CH2:9][C:10]#[N:11]>C(OCC)C>[ClH:7].[S:1]([NH:5][C:10](=[NH:11])[CH2:9][CH2:8][Cl:7])(=[O:3])(=[O:2])[NH2:4]

参加物

4

反応物 2

HCID 82267SulfamideHCID 867420433-Chloropropionitrile hydrogen chloride

生成物 1

HCID 178479209HCID 178479209、化合物

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒

実験手順

To a stirred suspension of 9.61 g. (0.10 mole) of sulfamide in 30 ml (34 g., 0.38 mole) of 3-chloropropionitrile hydrogen chloride gas is introduced, as described in Example 1. After cooling with ice water for one hour the reaction mixture is diluted with 30 ml of dry ethyl ether, the product is filtered off, washed twice with acetone and dried.

後処理

  1. additionTo a stirred suspension of 9.61 g
  2. filtrationthe product is filtered off
  3. washwashed twice with acetone
  4. customdried

出典と根拠

ORDレコード
ord-6ec711e95d084ee185c242200ab7ae81
出典データセット
uspto-grants-1989_05
特許番号
US04835281

関連ノート

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