Anthranilic Acid → 70346-37-1

HRID 1767148ノート

反応式

HRID 1767148 の反応式
[C:1]([OH:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[NH2:4].CO.[NH3:13]>>[C:1]([O-:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[NH2:4].[NH4+:13]

参加物

3

反応物 2

HCID 227Anthranilic AcidHCID 21705897Ammonia methanol

生成物 1

HCID 6736264670346-37-1収率 94%

実験手順

In a 50 mL volume glass vessel equipped with a stirrer and a thermometer were placed 5.0 g (36.5 mmol) of anthranilic acid and 20 mL (156 mmol) of 15 wt. % ammonia methanol solution. The reaction was carried out for 2 hours at room temperature. After the reaction was complete, the reaction mixture was concentrated under reduced pressure, to obtain 5.0 g (isolated yield: 94%) of ammonium anthranilate as white solid.

後処理

  1. customIn a 50 mL volume glass vessel equipped with a stirrer
  2. concentrationthe reaction mixture was concentrated under reduced pressure

出典と根拠

ORDレコード
ord-b7c18331578d4359a5aea05328154574
出典データセット
uspto-grants-2007_06
特許番号
US07232903B2

反応ノート

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