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HRID 1774334作成日:2026年10月26日

Myristyl bromide → 1-(4-Chlorophenyl)-3-tetradecyl imidazolium bromide

https://huagongshe.com/reaction/1774334

反応式

関与物質

役割名称HCID仕込み量
反応物Myristyl bromideHCID 8208—
反応物1-(4-Chlorophenyl)-1H-imidazoleHCID 142859—
溶媒TetrahydrofuranHCID 8028—
生成物1-(4-Chlorophenyl)-3-tetradecyl imidazolium bromideHCID 178443152—

反応手順

According to the general synthesis procedure 5.6 mmol (1.00 g) 1-(4-chlorophenyl)imidazole and 6.7 mmol (1.86 g, 1.82 ml) 1-bromotetradecane are dissolved in 5 ml THF and heated for 42 h to 90° C. At the end of the reaction the reaction mixture is cooled down to room temperature and the product is precipitated with diethylether.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09260397B2
出典データセットuspto-grants-2016_02
ORD IDord-102dde7402434d619b8f589ac226a8b0
出典メモuspto-grants-2016_02