化工社化工社 化学情報印刷レポート · 研究参考用
Myristyl bromide → 1-(4-Chlorophenyl)-3-tetradecyl imidazolium bromide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Myristyl bromide | HCID 8208 | — |
| 反応物 | 1-(4-Chlorophenyl)-1H-imidazole | HCID 142859 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | 1-(4-Chlorophenyl)-3-tetradecyl imidazolium bromide | HCID 178443152 | — |
反応手順
According to the general synthesis procedure 5.6 mmol (1.00 g) 1-(4-chlorophenyl)imidazole and 6.7 mmol (1.86 g, 1.82 ml) 1-bromotetradecane are dissolved in 5 ml THF and heated for 42 h to 90° C. At the end of the reaction the reaction mixture is cooled down to room temperature and the product is precipitated with diethylether.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09260397B2 |
| 出典データセット | uspto-grants-2016_02 |
| ORD ID | ord-102dde7402434d619b8f589ac226a8b0 |
| 出典メモ | uspto-grants-2016_02 |