HRID1774334

反应详情

EQUATION

反应方程式

HRID 1774334 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

According to the general synthesis procedure 5.6 mmol (1.00 g) 1-(4-chlorophenyl)imidazole and 6.7 mmol (1.86 g, 1.82 ml) 1-bromotetradecane are dissolved in 5 ml THF and heated for 42 h to 90° C. At the end of the reaction the reaction mixture is cooled down to room temperature and the product is precipitated with diethylether.

WORKUP

后处理

  1. temperatureheated for 42 h to 90° C
  2. customAt the end of the reaction the reaction mixture
  3. customthe product is precipitated with diethylether